(S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

Base Information

Chemical Name:(S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide
CAS No.:1253798-51-4
Molecular Formula:C₂₂H₂₇N₃O₈S
Molecular Weight:493.538
Hs Code.:

Synonyms:(S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

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Chemical Property of (S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

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Technology Process of (S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

There total 5 articles about (S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1253798-50-3
(2'RS,2S)-2-[2,3-dihydroxypropyl-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

: 1253798-51-4
(S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; for 1.5h;
DOI:10.1002/cmdc.201000230

Reference yield:

: 1253798-49-0
(S)-N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(2-nitrobenzenesulfonylamino)butyramide

: 1253798-51-4
(S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate / acetonitrile / 4.5 h / 20 - 50 °C

2: potassium osmate(VI) dihydrate; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 0 °C

3: sodium periodate / tetrahydrofuran; water / 1.5 h

With potassium osmate(VI) dihydrate; sodium periodate; N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In tetrahydrofuran; water; acetonitrile; tert-butyl alcohol;
DOI:10.1002/cmdc.201000230

Reference yield:

: 1253798-37-6
(S)-2-[allyl-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

: 1253798-51-4
(S)-2-[N-(2-oxoethyl)-(2-nitrobenzenesulfonyl)amino]-N-[2-(3,4-dimethoxyphenyl)ethyl]butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium osmate(VI) dihydrate; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 0 °C

2: sodium periodate / tetrahydrofuran; water / 1.5 h

With potassium osmate(VI) dihydrate; sodium periodate; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1002/cmdc.201000230