(R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

Base Information

Chemical Name:(R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate
CAS No.:1442649-65-1
Molecular Formula:C₂₄H₂₄O₄S
Molecular Weight:408.518
Hs Code.:

Synonyms:(R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

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Chemical Property of (R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

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Technology Process of (R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

There total 3 articles about (R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2444-37-3
methylsulfanyl-acetic acid

: 1442649-64-0
(R)-4-(hydroxy(naphthalen-2-yl)methyl)phenylisobutyrate

: 1442649-65-1
(R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja4034999

Reference yield:

: 120464-79-1
4-formylphenyl isobutyrate

: 1442649-65-1
(R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylzinc / toluene / 24 h / 65 °C / Inert atmosphere

1.2: 0.17 h / 0 °C / Inert atmosphere

1.3: 24 h / 0 °C / Inert atmosphere

2.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere

With dmap; diethylzinc; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1021/ja4034999

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1442649-65-1
(R)-4-((2-(methylthio)acetoxy)(naphthalen-2-yl)methyl)phenyl isobutyrate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere

2.1: diethylzinc / toluene / 24 h / 65 °C / Inert atmosphere

2.2: 0.17 h / 0 °C / Inert atmosphere

2.3: 24 h / 0 °C / Inert atmosphere

3.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere

With dmap; diethylzinc; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1021/ja4034999