11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

Base Information

Chemical Name:11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan
CAS No.:112999-93-6
Molecular Formula:C₂₅H₄₂O₄
Molecular Weight:406.606
Hs Code.:

Synonyms:11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

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Chemical Property of 11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

Chemical Property:

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Technology Process of 11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

There total 7 articles about 11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 52056-69-6
2-[(11-bromoundecyl)oxy]tetrahydro-2H-pyran

: 55359-65-4
1-methoxymethoxy-2-methylbenzene

: 112999-93-6
11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 112999-93-6
11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridinium-p-toluolsulfonat / CH₂Cl₂ / 18 h / Ambient temperature

2: 75 percent / 1.6 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 53463-68-6
1-bromo-10-decanol

: 112999-93-6
11-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>undecan

Guidance literature:: Multi-step reaction with 5 steps

2: 2.) LiAlH₄

3: 48 percent aqueous HBr / darkness

4: 96 percent / pyridinium-p-toluolsulfonat / CH₂Cl₂ / 18 h / Ambient temperature

5: 75 percent / 1.6 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

With lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen bromide; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;