1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.04,6]nonadec-7-ene-4-carbonyl]-amide

Base Information

Chemical Name:1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide
CAS No.:1044558-68-0
Molecular Formula:C₃₂H₄₀N₆O₇S
Molecular Weight:652.772
Hs Code.:

1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

Synonyms:1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

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Chemical Property of 1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

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Technology Process of 1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

There total 3 articles about 1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1044559-71-8
1-methyl-cyclopropanesulfonic acid [14-(4-methoxy-benzyl)-18-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

: 1044558-68-0
1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

Guidance literature:: 1-methyl-cyclopropanesulfonic acid [14-(4-methoxy-benzyl)-18-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 1044559-31-0
14-(4-methoxy-benzyl)-18-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carboxylic acid ethyl ester

: 1044558-68-0
1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; lithium hydroxide; water / tetrahydrofuran / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2.5 h / 20 °C

2.2: 20 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With methanol; lithium hydroxide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1044559-34-3
14-(4-methoxybenzyl)-18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carboxyric acid

: 1044558-68-0
1-methyl-cyclopropanesulfonic acid [18-(2-methoxy-6-phenylpyrimidin-4-yloxy)-2,15-dioxo-3,14,16-triaza-tricyclo[14.3.0.0*4,6*]nonadec-7-ene-4-carbonyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2.5 h / 20 °C

1.2: 20 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;