(E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

Base Information

Chemical Name:(E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone
CAS No.:102104-06-3
Molecular Formula:C₃₇H₃₂O₅
Molecular Weight:556.658
Hs Code.:

Synonyms:(E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

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Chemical Property of (E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

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Technology Process of (E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

There total 6 articles about (E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 102104-05-2
5-C-(o-Benzyloxybenzyl)-4-benzyloxy-6-hydroxy-2-methoxyacetophenone

: 100-52-7
benzaldehyde

: 102104-06-3
(E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

Guidance literature:: potassium hydroxide; In water; at 4 ℃; for 360h;
DOI:10.1016/S0040-4039(00)94957-8

Reference yield:

: 3602-54-8
4,6-dihydroxy-2-methoxyacetophenone

: 102104-06-3
(E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / ethanol / 4 h / Heating

2: 60 percent / H₂ / 10percent Pd/C

3: 10 percent / K₂CO₃ / acetone / 1.) reflux, 6 h, 2.) r.t., 16 h

4: 69 percent / KOH / H₂O / 360 h / 4 °C

With hydrogen; potassium carbonate; potassium hydroxide; palladium on activated charcoal; In ethanol; water; acetone;
DOI:10.1016/S0040-4039(00)94957-8

Reference yield:

: 20939-20-2
2-hydroxyphenyl-bis-1,1-piperidinomethane

: 102104-06-3
(E)-1-[4-Benzyloxy-3-(2-benzyloxy-benzyl)-2-hydroxy-6-methoxy-phenyl]-3-phenyl-propenone

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / ethanol / 4 h / Heating

2: 60 percent / H₂ / 10percent Pd/C

3: 10 percent / K₂CO₃ / acetone / 1.) reflux, 6 h, 2.) r.t., 16 h

4: 69 percent / KOH / H₂O / 360 h / 4 °C

With hydrogen; potassium carbonate; potassium hydroxide; palladium on activated charcoal; In ethanol; water; acetone;
DOI:10.1016/S0040-4039(00)94957-8