C₂₁H₂₃N₉O₄

Base Information

Chemical Name:C₂₁H₂₃N₉O₄
CAS No.:1325711-88-3
Molecular Formula:C₂₁H₂₃N₉O₄
Molecular Weight:465.472
Hs Code.:

C<sub>21</sub>H<sub>23</sub>N<sub>9</sub>O<sub>4</sub>

Synonyms:C₂₁H₂₃N₉O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₃N₉O₄

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Technology Process of C₂₁H₂₃N₉O₄

There total 6 articles about C₂₁H₂₃N₉O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1325711-77-0
C₂₁H₂₂N₆O₄

: 1325711-88-3
C₂₁H₂₃N₉O₄

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 0 - 90 ℃; for 10h;
DOI:10.1002/cmdc.201100126

Reference yield:

: 2004-06-0
6-Chloropurine riboside

: 1325711-88-3
C₂₁H₂₃N₉O₄

Guidance literature:: Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / acetone / 2 h / 20 °C

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 4 h / 40 °C / Inert atmosphere

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 50 °C

4: oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -78 °C

5: N-ethyl-N,N-diisopropylamine / propan-1-ol / 4 h / 70 °C

6: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 10 h / 0 - 90 °C

With sodium azide; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; benzotriazol-1-ol; toluene-4-sulfonic acid; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In propan-1-ol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/cmdc.201100126

Reference yield:

: 1325711-76-9
C₁₃H₁₂ClN₅O₃

: 1325711-88-3
C₂₁H₂₃N₉O₄

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / propan-1-ol / 4 h / 70 °C

2: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 10 h / 0 - 90 °C

With sodium azide; ammonium chloride; N-ethyl-N,N-diisopropylamine; In propan-1-ol; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201100126