1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline

Base Information

• Chemical Name: 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline
• CAS No.: 1085708-83-3
• Molecular Formula: C₂₁H₁₇N₅OS
• Molecular Weight: 387.465

Synonyms:1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline

Chemical Property of 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline

Chemical Property:

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Technology Process of 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline

There total 1 articles about 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

carbon disulfide (75-15-0,12122-00-8) + 1-[4-(N,N-dimethylamino)phenyl]-β-carboline-3-carboxylic acid hydrazide (1085709-11-0) → 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline (1085708-83-3)

Guidance literature:

With potassium hydroxide; In ethanol; for 48h; Reflux;

DOI:10.1016/j.bmc.2008.10.008

Reference yield: 92.0%

pyrrolidine (123-75-1) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline (1085708-83-3) → 1-(4-(N,N-dimethylamino)phenyl)-3-[3-(pyrrolidin-1-ylmethyl)-2-thioxo-1,3,4-oxadiazol-5-yl]-β-carboline (1252605-89-2)

Guidance literature:

In ethanol; at 60 ℃;

DOI:10.1590/S0103-50532010000200014

Reference yield: 92.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-(4-N,N-dimethylaminophenyl)-3-(2-thioxo-1,3,4-oxadiazol-5-yl) β-carboline (1085708-83-3) + N-butylamine (109-73-9,85404-21-3) → 1-(4-(N,N-dimethylamino)phenyl)-3-[3-(butylaminomethyl)-2-thioxo-1,3,4-oxadiazol-5-yl]-β-carboline (1252605-86-9)

Guidance literature:

In ethanol; at 60 ℃;

DOI:10.1590/S0103-50532010000200014

upstream raw materials:

carbon disulfide

1-[4-(N,N-dimethylamino)phenyl]-β-carboline-3-carboxylic acid hydrazide

Downstream raw materials:

1-(4-N,N-dimethylaminophenyl)-3-(4-amino-5-thioxo-1,2,4-triazol-3-yl) β-carboline

1-(4-N,N-dimethylaminophenyl)-3-(2-methylthio-1,3,4-oxadiazol-5-yl) β-carboline

1-(4-(N,N-dimethylamino)phenyl)-3-[3-(pyrrolidin-1-ylmethyl)-2-thioxo-1,3,4-oxadiazol-5-yl]-β-carboline

1-(4-(N,N-dimethylamino)phenyl)-3-[3-(morpholin-4-ylmethyl)-2-thioxo-1,3,4-oxadiazol-5-yl]-β-carboline

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