methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

Base Information

Chemical Name:methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate
CAS No.:1313739-85-3
Molecular Formula:C₂₀H₂₀N₂O₂
Molecular Weight:320.391
Hs Code.:

Synonyms:methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

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Chemical Property of methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

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Technology Process of methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

There total 5 articles about methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1313739-62-6
methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

: 1313739-84-2
methyl 2-benzyl-4-methyl-2,4-dihydropyrrolo[3,4-b]indole-3-carboxylate

: 1313739-85-3
methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In tetrahydrofuran; at 110 ℃; for 72h; sealed tube;
DOI:10.1039/c1ob05087g

Reference yield:

: C₁₃H₁₃IN₂O₂

: 1313739-84-2
methyl 2-benzyl-4-methyl-2,4-dihydropyrrolo[3,4-b]indole-3-carboxylate

: 1313739-85-3
methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 24 h / 20 °C

2: potassium carbonate / acetonitrile / 2.5 h / 55 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / 72 h / 110 °C / sealed tube

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tris(acetoxy)borohydride; potassium carbonate; caesium carbonate; In tetrahydrofuran; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c1ob05087g

Reference yield:

: C₁₃H₁₅IN₂O₂

: 1313739-84-2
methyl 2-benzyl-4-methyl-2,4-dihydropyrrolo[3,4-b]indole-3-carboxylate

: 1313739-85-3
methyl 2-benzyl-4-methyl-1,2,3,4-tetrahydropyrrolo[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 2.5 h / 55 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / 72 h / 110 °C / sealed tube

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; caesium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c1ob05087g