methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

Base Information

Chemical Name:methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate
CAS No.:1313739-62-6
Molecular Formula:C₂₀H₂₁IN₂O₂
Molecular Weight:448.303
Hs Code.:

Synonyms:methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

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Chemical Property of methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

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Technology Process of methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

There total 4 articles about methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₅IN₂O₂

: 100-39-0
benzyl bromide

: 1313739-62-6
methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 55 ℃; for 2.5h;
DOI:10.1039/c1ob05087g

Reference yield:

: C₁₃H₁₃IN₂O₂

: 1313739-62-6
methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 24 h / 20 °C

2: potassium carbonate / acetonitrile / 2.5 h / 55 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c1ob05087g

Reference yield:

: 1313739-57-9
2-iodo-1-methyl-1H-indole-3-carbaldehyde

: 1313739-62-6
methyl 2-{N-benzyl-N-[(2-iodo-1-methyl-1H-indol-3-yl)methyl]amino}acetate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; triethylamine / 1,2-dichloro-ethane / 0.17 h / 20 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 24 h / 20 °C

3: potassium carbonate / acetonitrile / 2.5 h / 55 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; triethylamine; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c1ob05087g