methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

Base Information

Chemical Name:methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal
CAS No.:332843-98-8
Molecular Formula:C₃₁H₄₀O₆Si
Molecular Weight:536.74
Hs Code.:

Synonyms:methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

Suppliers and Price of methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

Chemical Property:

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Technology Process of methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

There total 4 articles about methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 332843-96-6
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

: 332843-98-8
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

: 332843-97-7
(S)-4-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-3-(2-trimethylsilanyl-ethoxymethoxy)-butan-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.129

Reference yield:

: 332843-97-7
(S)-4-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-3-(2-trimethylsilanyl-ethoxymethoxy)-butan-1-ol

: 332843-98-8
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve;
DOI:10.1016/S0040-4039(00)02260-7

Reference yield:

: 332843-95-5
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-hydroxybutanoate

: 332843-98-8
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / i-Pr₂NEt

2: DIBAL-H

3: TPAP; NMO; 4 Angstroem sieves

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine;
DOI:10.1016/S0040-4039(00)02260-7