methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

Base Information

Chemical Name:methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate
CAS No.:332843-96-6
Molecular Formula:C₃₂H₄₂O₇Si
Molecular Weight:566.767
Hs Code.:

Synonyms:methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

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Technology Process of methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

There total 2 articles about methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 332843-95-5
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-hydroxybutanoate

: 332843-96-6
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine;
DOI:10.1016/S0040-4039(00)02260-7

Reference yield:

: 617-55-0
dimethyl (S)-malate

: 332843-96-6
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: BH₃*DMS; NaBH₄

2: i-Pr₂NEt

3: 100 percent / i-Pr₂NEt

With sodium tetrahydroborate; dimethylsulfide borane complex; N-ethyl-N,N-diisopropylamine;
DOI:10.1016/S0040-4039(00)02260-7

Reference yield: 75.0%

: 332843-96-6
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanoate

: 332843-98-8
methyl (3S)-4-(4,4'-dimethoxytriphenyl)methoxy-3-(2-trimethylsilylethoxy)methoxybutanal

: 332843-97-7
(S)-4-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-3-(2-trimethylsilanyl-ethoxymethoxy)-butan-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.129