3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

Base Information

Chemical Name:3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester
CAS No.:160726-36-3
Molecular Formula:C₂₄H₂₆O₆
Molecular Weight:410.467
Hs Code.:

Synonyms:3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

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Chemical Property of 3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

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Technology Process of 3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

There total 3 articles about 3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 160726-35-2
3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

: 115-11-7,15220-85-6
isobutene

: 160726-36-3
3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

Guidance literature:: With sulfuric acid; In dichloromethane; for 6h;

Reference yield:

: 129866-90-6
2,2'-dimethoxy-5,5'-diformyl-diphenyl-iodonium bromide

: 160726-36-3
3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaOMe / 1.) MeOH, 2.) DME, reflux, 72 h

2: 75 percent / piperidine / pyridine / 1.67 h / 100 °C

3: 95 percent / H₂SO₄ / CH₂Cl₂ / 6 h

With piperidine; sulfuric acid; sodium methylate; In pyridine; dichloromethane;

Reference yield:

: 160726-34-1
methyl 3-<4-(2-methoxy-5-formylphenoxy)-phenyl>-2-propenoate

: 160726-36-3
3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / piperidine / pyridine / 1.67 h / 100 °C

2: 95 percent / H₂SO₄ / CH₂Cl₂ / 6 h

With piperidine; sulfuric acid; In pyridine; dichloromethane;