Technology Process of C13H12N6O
There total 4 articles about C13H12N6O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide; ammonium chloride;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 1h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/jo400372c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium hydroxide / water; ethanol / 2 h / Reflux
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 18 h / 20 °C
3: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 1 h / 110 °C / Inert atmosphere; Sealed tube
With
sodium azide; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo400372c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 18 h / 20 °C
2: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 1 h / 110 °C / Inert atmosphere; Sealed tube
With
sodium azide; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
DOI:10.1021/jo400372c
