(E)-2-Pyrimidinecarboxaldehyde oxime

Base Information

• Chemical Name: (E)-2-Pyrimidinecarboxaldehyde oxime
• CAS No.: 39232-40-1
• Molecular Formula: C5H5 N3 O
• Molecular Weight: 123.114
• Hs Code.: 2933599090
• Mol file: 39232-40-1.mol

Synonyms:2-Pyrimidinecarboxaldehyde,oxime, (E)- (9CI); syn-Pyrimidine-2-aldoxime

Chemical Property of (E)-2-Pyrimidinecarboxaldehyde oxime

Chemical Property:

• Boiling Point: 349.8±25.0 °C(Predicted)
• PKA: 9.29±0.10(Predicted)
• PSA: 58.37000
• Density: 1.28
• LogP: 0.28470
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

(E)-Pyrimidine-2-carbaldehydeoxime 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-2-Pyrimidinecarboxaldehyde oxime

There total 2 articles about (E)-2-Pyrimidinecarboxaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.2%

2-(Diethoxymethyl)pyrimidine → pyrimidin-2-carbaldehyde oxime (39232-40-1)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; water; at 60 ℃;

Reference yield:

→ pyrimidin-2-carbaldehyde oxime (39232-40-1)

Guidance literature:

2-Formylpyrimidin, Hydroxylaminhydrochlorid;

DOI:10.1007/BF00475549

Reference yield: 63.0%

pyrimidin-2-carbaldehyde oxime (39232-40-1) → 2-cyanopyrimidine (14080-23-0)

Guidance literature:

With Burgess Reagent; In dichloromethane; at 25 ℃; for 2h;

DOI:10.1080/00397910008087179

Downstream raw materials:

2-cyanopyrimidine