N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

Base Information

Chemical Name:N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester
CAS No.:178059-31-9
Molecular Formula:C₃₃H₃₅N₃O₅
Molecular Weight:553.658
Hs Code.:

Synonyms:N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

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Chemical Property of N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

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Technology Process of N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

There total 6 articles about N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 135942-02-8
N^α-benzyl-N^α-Z hydrazine

: 157223-28-4
((R)-1-(S)-Oxiranyl-2-phenyl-ethyl)-carbamic acid benzyl ester

: 178059-31-9
N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: In isopropyl alcohol; for 48h; Heating;
DOI:10.1016/j.bmcl.2005.08.093

Reference yield:

: 63219-70-5
N-(benzyloxycarbonyl)-D-phenylalaninal

: 178059-31-9
N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / 1.) -78 deg C, 2 h 2.) RT, 0.5 h

2: 2.7 g / m-chloroperbenzoic acid / CH₂Cl₂ / Ambient temperature

3: 72 percent / propan-2-ol / 24 h / Heating

4: trifluoroacetic acid / CH₂Cl₂

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; isopropyl alcohol; toluene;
DOI:10.1021/jm9507183

Reference yield:

: 95832-30-7
N-<(benzyloxy)carbonyl>-(2R)-amino-1-phenylbut-3-ene

: 178059-31-9
N'-Benzyl-N'-((2R,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 2.7 g / m-chloroperbenzoic acid / CH₂Cl₂ / Ambient temperature

2: 72 percent / propan-2-ol / 24 h / Heating

3: trifluoroacetic acid / CH₂Cl₂

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; isopropyl alcohol;
DOI:10.1021/jm9507183