C₄₈H₅₆O₁₃

Base Information

Chemical Name:C₄₈H₅₆O₁₃
CAS No.:264132-59-4
Molecular Formula:C₄₈H₅₆O₁₃
Molecular Weight:840.965
Hs Code.:

C<sub>48</sub>H<sub>56</sub>O<sub>13</sub>

Synonyms:C₄₈H₅₆O₁₃

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Chemical Property of C₄₈H₅₆O₁₃

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Technology Process of C₄₈H₅₆O₁₃

There total 11 articles about C₄₈H₅₆O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 264132-56-1
C₅₀H₅₇Cl₃O₁₃

: 264132-59-4
C₄₈H₅₆O₁₃

Guidance literature:: With phosphate buffer; zinc; In tetrahydrofuran; water; for 4h;
DOI:10.1021/jo991681n

Reference yield:

: 264132-38-9
(1R,2S)-[2-(p-methoxybenzyloxymethoxy)-1-ethenylpropoxy]acetic acid tert-butyl ester

: 264132-59-4
C₄₈H₅₆O₁₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: ozone; Ph₃P / CH₂Cl₂ / -78 °C

1.2: 65 percent / CuI; n-Bu₃P; BuLi / diethyl ether; tetrahydrofuran; hexane / 2 h / -78 °C

2.1: trifluoroacetic acid / benzene / 0.5 h / Heating

2.2: LiHMDS; Me₃SiCl; Et₃N / tetrahydrofuran / -78 °C

2.3: 89 percent / HCl / H₂O / pH 2

3.1: 92 percent / DMAP; DIC; TFA / CH₂Cl₂ / 40 °C

4.1: 82 percent / DDQ / H₂O; CH₂Cl₂ / 1 h

5.1: 96 percent / imidazole / dimethylformamide / 8 h / 20 °C

6.1: 100 percent / lithium hydroxide / 2-methyl-propan-2-ol; H₂O / 2 h

7.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

7.2: 92 percent / DMAP / benzene / 2 h

8.1: 100 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

9.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

9.2: 95 percent / DMAP; Et₃N / benzene / 2 h

10.1: 95 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

11.1: 95 percent / phosphate buffer; zinc dust / H₂O; tetrahydrofuran / 4 h

With 1H-imidazole; dmap; lithium hydroxide; phosphate buffer; 2,4,6-trichlorobenzoyl chloride; hydrogen fluoride; ozone; dacarbazine; triethylamine; triphenylphosphine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; benzene; 1.1: Oxidation / 1.2: Addition / 2.1: Cyclization / 2.2: Rearrangement / 2.3: Hydrolysis / 3.1: Esterification / 4.1: Hydrolysis / 5.1: Etherification / 6.1: Hydrolysis / 7.1: Substitution / 7.2: Substitution / 8.1: Hydrolysis / 9.1: Substitution / 9.2: Substitution / 10.1: Hydrolysis / 11.1: Reduction;
DOI:10.1021/jo991681n

Reference yield:

: 264132-42-5
(2S,3S,6R)-6-[(1S)-1-hydroxyethyl]-3-benzyloxymethyl-3,6-dihydro-2H-pyran-2-carboxylic acid 2,2,2-trichloroethyl ester

: 264132-59-4
C₄₈H₅₆O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: 96 percent / imidazole / dimethylformamide / 8 h / 20 °C

2.1: 100 percent / lithium hydroxide / 2-methyl-propan-2-ol; H₂O / 2 h

3.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

3.2: 92 percent / DMAP / benzene / 2 h

4.1: 100 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

5.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

5.2: 95 percent / DMAP; Et₃N / benzene / 2 h

6.1: 95 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

7.1: 95 percent / phosphate buffer; zinc dust / H₂O; tetrahydrofuran / 4 h

With 1H-imidazole; lithium hydroxide; phosphate buffer; 2,4,6-trichlorobenzoyl chloride; hydrogen fluoride; triethylamine; zinc; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 1.1: Etherification / 2.1: Hydrolysis / 3.1: Substitution / 3.2: Substitution / 4.1: Hydrolysis / 5.1: Substitution / 5.2: Substitution / 6.1: Hydrolysis / 7.1: Reduction;
DOI:10.1021/jo991681n