2,2'-trithio

Base Information

Chemical Name:2,2'-trithio
CAS No.:117088-94-5
Molecular Formula:C₂₄H₃₀N₄O₂S₃
Molecular Weight:502.726
Hs Code.:

2,2'-trithio<N-(cyclohexyl)-3-pyridinecarboxamide>

Synonyms:2,2'-trithio

Suppliers and Price of 2,2'-trithio

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-trithio

Chemical Property:

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Technology Process of 2,2'-trithio

There total 6 articles about 2,2'-trithio which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 117088-90-1
2,2'-trithiobis(3-pyridinecarbonyl chloride)

: 117088-94-5
2,2'-trithio

Guidance literature:: With triethylamine; In chloroform; at 0 ℃; for 4h;
DOI:10.1002/jhet.5570250103

Reference yield:

: 104857-34-3
2,2'-dithiobis(3-pyridinecarbonyl chloride)

: 117088-94-5
2,2'-trithio

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / pyridine / 1 h / Ambient temperature

2: 50 percent / 1M aq. NaOH / methanol / 24 h / Ambient temperature

3: 70 percent / sulfur dichloride, pyridine / CHCl₃ / 9 h / Ambient temperature

4: 72 percent / SOCl₂, pyridine / CH₂Cl₂ / 0.5 h / 0 °C

5: 75 percent / triethylamine / CHCl₃ / 4 h / 0 °C

With pyridine; sodium hydroxide; thionyl chloride; sulfur dichloride; triethylamine; In methanol; dichloromethane; chloroform;
DOI:10.1002/jhet.5570250103

Reference yield:

: 38521-46-9
1,2-dihydro-2-thioxo-3-pyridine carboxylic scid

: 117088-94-5
2,2'-trithio

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / sulfur dichloride, pyridine / CHCl₃ / 9 h / Ambient temperature

2: 72 percent / SOCl₂, pyridine / CH₂Cl₂ / 0.5 h / 0 °C

3: 75 percent / triethylamine / CHCl₃ / 4 h / 0 °C

With pyridine; thionyl chloride; sulfur dichloride; triethylamine; In dichloromethane; chloroform;
DOI:10.1002/jhet.5570250103