difluoro-(4-formylphenyl)acetic acid ethyl ester

Base Information

Chemical Name:difluoro-(4-formylphenyl)acetic acid ethyl ester
CAS No.:936352-93-1
Molecular Formula:C₁₁H₁₀F₂O₃
Molecular Weight:228.195
Hs Code.:

Synonyms:difluoro-(4-formylphenyl)acetic acid ethyl ester

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Chemical Property of difluoro-(4-formylphenyl)acetic acid ethyl ester

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Technology Process of difluoro-(4-formylphenyl)acetic acid ethyl ester

There total 7 articles about difluoro-(4-formylphenyl)acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.3%

: 667-27-6
Ethyl bromodifluoroacetate

: 100-52-7
benzaldehyde

: 936352-93-1
difluoro-(4-formylphenyl)acetic acid ethyl ester

Guidance literature:: With tris[2-phenylpyridinato-C₂,N]iridium(III); 1,10-Phenanthroline; caesium carbonate; In n-heptane; at 25 ℃; for 24h; Irradiation;

Reference yield: 74.0%

: 667-27-6
Ethyl bromodifluoroacetate

: 94839-07-3
3,4-(methylenedioxy)-benzeneboronic acid

: 936352-93-1
difluoro-(4-formylphenyl)acetic acid ethyl ester

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 80 ℃; for 24h; Reagent/catalyst; Schlenk technique; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.201309535

Reference yield:

: 667-27-6
Ethyl bromodifluoroacetate

: 100-52-7
benzaldehyde

: 936352-93-1
difluoro-(4-formylphenyl)acetic acid ethyl ester

: C₁₁H₁₀F₂O₃

: C₁₁H₁₀F₂O₃

Guidance literature:: With fac-tris[2-phenylpyridinato-C²,N]iridium(III); potassium acetate; In methanol; at 20 ℃; for 18h; Reagent/catalyst; Solvent; Overall yield = 63 percent; Overall yield = 13.5 mg; regioselective reaction; Inert atmosphere; Schlenk technique; Irradiation;
DOI:10.1039/c9cc09586a