Technology Process of C35H27BO2
There total 6 articles about C35H27BO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C35H25Br;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
Inert atmosphere;
Trimethyl borate;
In
tetrahydrofuran; hexane;
at 20 ℃;
With
hydrogenchloride; water;
In
tetrahydrofuran; hexane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / 120 °C
2.1: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere
3.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
3.2: 20 °C
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 2 h / 120 °C
5.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
5.2: 20 °C
With
N-Bromosuccinimide; n-butyllithium; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
1.2: 20 °C
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 2 h / 120 °C
3.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
3.2: 20 °C
With
n-butyllithium; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; water; toluene;