Succinic acid benzyl ester phenylsulfanylmethyl ester

Base Information

Chemical Name:Succinic acid benzyl ester phenylsulfanylmethyl ester
CAS No.:201210-68-6
Molecular Formula:C₁₈H₁₈O₄S
Molecular Weight:330.405
Hs Code.:

Synonyms:Succinic acid benzyl ester phenylsulfanylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Succinic acid benzyl ester phenylsulfanylmethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Succinic acid benzyl ester phenylsulfanylmethyl ester

There total 1 articles about Succinic acid benzyl ester phenylsulfanylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7205-91-6
phenylthiomethyl chloride

: 103-40-2
succinic acid monobenzyl ester

: 201210-68-6
Succinic acid benzyl ester phenylsulfanylmethyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; 1.) room temperature, 30 min; 70 deg C, 15 min, 2.) room temperature, 3 h; 70 deg C, 15 min;
DOI:10.1021/jo971076p

Reference yield:

: 201210-68-6
Succinic acid benzyl ester phenylsulfanylmethyl ester

: 201210-74-4
Succinic acid 5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) SO₂Cl₂, 2.) cis-4-cyclohexene-1,2-dicarboxylic acid / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 1 h

2: 76 percent / Et₃N / dimethylformamide / 16 h / Ambient temperature

3: 99 percent / 1,4-cyclohexadiene / Pd/C / acetic acid / 1 h / Ambient temperature

4: 43 percent / EDCI*HCl / dimethylformamide / 2 h / Ambient temperature

With sulfuryl dichloride; cyclohexa-1,4-diene; cis-1,2,3,6-tetrahydrophthalic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo971076p

Reference yield:

: 201210-68-6
Succinic acid benzyl ester phenylsulfanylmethyl ester

: 201210-70-0
succinic acid benzyl ester (5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) SO₂Cl₂, 2.) cis-4-cyclohexene-1,2-dicarboxylic acid / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 1 h

2: 76 percent / Et₃N / dimethylformamide / 16 h / Ambient temperature

With sulfuryl dichloride; cis-1,2,3,6-tetrahydrophthalic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jo971076p