benzyl-amidophosphoric acid

Base Information

Chemical Name:benzyl-amidophosphoric acid
CAS No.:98334-26-0
Molecular Formula:C₇H₁₀NO₃P
Molecular Weight:187.135
Hs Code.:

Synonyms:benzyl-amidophosphoric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl-amidophosphoric acid

Chemical Property:

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Technology Process of benzyl-amidophosphoric acid

There total 4 articles about benzyl-amidophosphoric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 53640-96-3
diethyl N-benzylphosphoramidate

: 98334-26-0
benzyl-amidophosphoric acid

Guidance literature:: With trimethylsilyl bromide; In acetonitrile; at 40 ℃; for 0.166667h; microwave irradiation;
DOI:10.1016/j.tetlet.2006.06.126

Reference yield:

: 33985-75-0
phosphoramidic acid, N-(phenylmethyl)-, diphenyl ester

: 98334-26-0
benzyl-amidophosphoric acid

Guidance literature:: With potassium hydroxide;
DOI:10.1021/ja00745a032

Reference yield:

: 100-46-9
benzylamine

: 98334-26-0
benzyl-amidophosphoric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

2: 93 percent / trimethylsilyl bromide / acetonitrile / 0.17 h / 40 °C / microwave irradiation

With trimethylsilyl bromide; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2006.06.126