2-carbethoxybenzyl tellurocyanate

Base Information

Chemical Name:2-carbethoxybenzyl tellurocyanate
CAS No.:78763-93-6
Molecular Formula:C₁₁H₁₁NO₂Te
Molecular Weight:316.814
Hs Code.:

Synonyms:2-carbethoxybenzyl tellurocyanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-carbethoxybenzyl tellurocyanate

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Technology Process of 2-carbethoxybenzyl tellurocyanate

There total 7 articles about 2-carbethoxybenzyl tellurocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 64-17-5
ethanol

: 151-50-8
potassium cyanide

: 78763-92-5
<2-(iodocarbonyl)benzyl>telluryl iodide

: 78763-93-6
2-carbethoxybenzyl tellurocyanate

Guidance literature:: In dimethyl sulfoxide; for 0.5h;
DOI:10.1021/jo00334a017

Reference yield: 33.0%

: 64-17-5
ethanol

: 151-50-8
potassium cyanide

: 78763-90-3
<2-(chlorocarbonyl)benzyl>telluryl chloride

: 78763-93-6
2-carbethoxybenzyl tellurocyanate

Guidance literature:: In dimethyl sulfoxide; for 0.5h;
DOI:10.1021/jo00334a017

Reference yield:

: 7115-90-4
α-Bromo-o-toluyl Chloride

: 78763-93-6
2-carbethoxybenzyl tellurocyanate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium borohydride, tellurium, 2.) Adogen 464 / 1.) water, 40 deg C, 15 min, 2.) toluene, 50 deg C, 30 min,

2: 84 percent / sulfuryl chloride / CCl₄ / 0.5 h / -23 °C

3: 33 percent / dimethylsulfoxide / 0.5 h

With tellurium; sodium tetrahydroborate; sulfuryl dichloride; adogen 464; In tetrachloromethane; dimethyl sulfoxide;
DOI:10.1021/jo00334a017