(Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

Base Information

Chemical Name:(Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol
CAS No.:76579-70-9
Molecular Formula:C₂₇H₃₁NO₂
Molecular Weight:401.549
Hs Code.:

Synonyms:(Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

Suppliers and Price of (Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

Chemical Property:

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Technology Process of (Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

There total 3 articles about (Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4584-46-7
(2-chloroethyl)dimethylamine hydrochloride

: 1,1-bis(4-hydroxyphenyl)-2-phenylpent-1-ene

: 76579-70-9
(Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

: C₂₇H₃₁NO₂

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 2.5h; Overall yield = 51 %; Overall yield = 0.2 g; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.bmc.2017.01.019

Reference yield:

: 611-99-4
4,4'-Dihydroxybenzophenone

: 76579-70-9
(Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

: C₂₇H₃₁NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; titanium tetrachloride / tetrahydrofuran / 2.5 h / Inert atmosphere; Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 2.5 h / Inert atmosphere

With titanium tetrachloride; caesium carbonate; zinc; In tetrahydrofuran; N,N-dimethyl-formamide; 1: |McMurry Reaction;
DOI:10.1016/j.bmc.2017.01.019

Reference yield:

: 495-40-9
propiophenone

: 76579-70-9
(Z)-4-[1-[4-(2-dimethylamino-ethoxy)-phenyl]-4-methyl-2-phenyl-pent-1-enyl]phenol

: C₂₇H₃₁NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; titanium tetrachloride / tetrahydrofuran / 2.5 h / Inert atmosphere; Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 2.5 h / Inert atmosphere

With titanium tetrachloride; caesium carbonate; zinc; In tetrahydrofuran; N,N-dimethyl-formamide; 1: |McMurry Reaction;
DOI:10.1016/j.bmc.2017.01.019