dimethylphenyl sulfonium tetrafluoroborate

Base Information

• Chemical Name: dimethylphenyl sulfonium tetrafluoroborate
• CAS No.: 33613-52-4
• Molecular Formula: BF₄*C₈H₁₁S
• Molecular Weight: 226.046
• Mol file: 33613-52-4.mol

Synonyms:dimethylphenyl sulfonium tetrafluoroborate

Chemical Property of dimethylphenyl sulfonium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dimethylphenyl sulfonium tetrafluoroborate

There total 3 articles about dimethylphenyl sulfonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

methyl-phenyl-thioether (100-68-5) + methyl iodide (74-88-4) → dimethylphenyl sulfonium tetrafluoroborate (33613-52-4)

Guidance literature:

With silver tetrafluoroborate; In acetonitrile;

DOI:10.1021/ja00280a033

Reference yield:

methyl-phenyl-thioether (100-68-5) + trimethoxonium tetrafluoroborate (420-37-1) → dimethylphenyl sulfonium tetrafluoroborate (33613-52-4)

Guidance literature:

In N,N-dimethyl-formamide; Equilibrium constant; other solvents; methyl transfer between substituted phenylmethyl thioesters and Me₃O⁺BF₄^-;

DOI:10.1021/jo961658r

Reference yield:

methyl-phenyl-thioether (100-68-5) + 1-decenyl(phenyl)(tetrafluoroborato)-λ3-iodane (102987-32-6) → dimethylphenyl sulfonium tetrafluoroborate (33613-52-4) + dec-1-yn-1-yl(phenyl)sulfane (160985-71-7)

Guidance literature:

In dichloromethane; for 47h; Heating;

DOI:10.1039/b212512a

upstream raw materials:

methyl-phenyl-thioether

trimethoxonium tetrafluoroborate

methyl iodide

1-decenyl(phenyl)(tetrafluoroborato)-λ³-iodane

Downstream raw materials:

methyl-phenyl-thioether

C₂₃H₁₆F₃NS

C₁₈H₁₄F₃NS

N-methoxy-N-methylbenzamide