3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

Base Information

Chemical Name:3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether
CAS No.:623124-95-8
Molecular Formula:C₂₄H₂₇N₄OP
Molecular Weight:418.478
Hs Code.:

Synonyms:3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

Suppliers and Price of 3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

There total 1 articles about 3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 208105-69-5
3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl)propan-1-ol

: 74-88-4
methyl iodide

: 623124-95-8
3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

Guidance literature:: With potassium tert-butylate; potassium iodide; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/ejic.200200535

Reference yield: 91.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 623124-95-8
3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

: 623125-27-9
CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiBr₂

Guidance literature:: In tetrahydrofuran; (Ar), ligand in THF added rapidly to Ni complex in THF, stirred at 25°C for 12 h; evapd.(vac.), washed (diethyl ether), dried (vac.), recrystd.(CH2Cl2/Et2O), elem. anal.;
DOI:10.1002/ejic.200200535

Reference yield: 88.0%

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: 623124-95-8
3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

: 623125-30-4
CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiCl₂

Guidance literature:: In tetrahydrofuran; (Ar), ligand in THF added rapidly to Ni complex in THF, stirred at 25°C for 12 h; evapd.(vac.), washed (diethyl ether), dried (vac.), recrystd.(CH2Cl2/Et2O), elem. anal.;
DOI:10.1002/ejic.200200535