N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

Base Information

Chemical Name:N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide
CAS No.:1342283-83-3
Molecular Formula:C₂₀H₂₅NO₅
Molecular Weight:359.422
Hs Code.:

Synonyms:N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

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Chemical Property of N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

Chemical Property:

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Technology Process of N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

There total 3 articles about N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1078-61-1
dihydrocaffeic acid

: 1016670-95-3
2-methoxy-4-[(propylamino)methyl]phenol

: 1342283-83-3
N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

Guidance literature:: dihydrocaffeic acid; With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

2-methoxy-4-[(propylamino)methyl]phenol; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.foodchem.2011.08.021

Reference yield:

: 92834-90-7
C₁₁H₁₅NO₂

: 1342283-83-3
N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol / 3 h

2.1: triethylamine / N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 2 h / 20 °C

With sodium tetrahydroborate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.foodchem.2011.08.021

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1342283-83-3
N-propyl-N-(3-methoxy-4-hydroxybenzyl)-3-(3,4-dihydroxyphenyl)propanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 3 h

2.1: sodium tetrahydroborate / methanol / 3 h

3.1: triethylamine / N,N-dimethyl-formamide / 0.5 h / 0 °C

3.2: 2 h / 20 °C

With sodium tetrahydroborate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.foodchem.2011.08.021