1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

Base Information

Chemical Name:1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil
CAS No.:1290140-53-2
Molecular Formula:C₅₄H₈₂N₄O₆
Molecular Weight:883.268
Hs Code.:

Synonyms:1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

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Chemical Property of 1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

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Technology Process of 1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

There total 11 articles about 1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1091632-52-8
1-hexyl-6-iodo-2,4(1H,3H)-pyrimidinedione

: 152270-00-3
1,4-bis(dodecyloxy)-2,5-diethynylbenzene

: 1290140-53-2
1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja2011516

Reference yield: 40.3%

: 1091632-54-0
C₁₂H₁₆N₂O₂

: 145483-66-5
1,4-bis(dodecyloxy)-2,5-diiodobenzene

: 1290140-53-2
1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; for 12h; Inert atmosphere;
DOI:10.1039/c3nj01606d

Reference yield:

: 3230-09-9
1,4-bis-dodecyloxy-benzene

: 1290140-53-2
1,1'-hexyl-6,6'-[(1,4-bis(dodecyloxy)-2,5-phenylene)diethynyl]bisuracil

Guidance literature:: Multi-step reaction with 4 steps

1: mercury(II) diacetate; iodine / dichloromethane / 12 h / 20 °C

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

3: methanol; potassium hydroxide / tetrahydrofuran; water / 1 h / 20 °C

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With methanol; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; mercury(II) diacetate; iodine; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/ja2011516