C₃₉H₅₄N₂O₁₀

Base Information

Chemical Name:C₃₉H₅₄N₂O₁₀
CAS No.:915782-52-4
Molecular Formula:C₃₉H₅₄N₂O₁₀
Molecular Weight:710.865
Hs Code.:

C<sub>39</sub>H<sub>54</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:C₃₉H₅₄N₂O₁₀

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Chemical Property of C₃₉H₅₄N₂O₁₀

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Technology Process of C₃₉H₅₄N₂O₁₀

There total 10 articles about C₃₉H₅₄N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 123-75-1
pyrrolidine

: C₄₁H₅₁NO₁₀S

: 915782-52-4
C₃₉H₅₄N₂O₁₀

Guidance literature:: In benzene; at 20 ℃;
DOI:10.1016/j.tetlet.2006.08.115

Reference yield:

: 915782-46-6
1-benzyloxy-oct-7-yn-4-one

: 915782-52-4
C₃₉H₅₄N₂O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1: TsOH / benzene / Heating

2: 78 percent / nBuLi; MgBr₂ / tetrahydrofuran / -78 - 0 °C

3: 75 percent / tBuLi; CuBr*Me₂S / tetrahydrofuran / -78 °C

4: 85 percent / MeLi / tetrahydrofuran / -78 °C

5: 84 percent / Zn(Cu) / tetrahydrofuran / -45 °C

6: 87 percent / nBu₃SnH; Et₃B / benzene / Heating

7: 85 percent / p-TsOH / acetone / 20 °C

8: 88 percent / benzene / 20 °C

With n-butyllithium; zinc copper; copper(I) bromide dimethylsulfide complex; triethyl borane; methyllithium; tert.-butyl lithium; tri-n-butyl-tin hydride; toluene-4-sulfonic acid; magnesium bromide; In tetrahydrofuran; acetone; benzene; 5: Marino annulation reaction;
DOI:10.1016/j.tetlet.2006.08.115

Reference yield:

: 915782-47-7
2-(3-benzyloxy-propyl)-2-but-3-ynyl-[1,3]dioxolane

: 915782-52-4
C₃₉H₅₄N₂O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / nBuLi; MgBr₂ / tetrahydrofuran / -78 - 0 °C

2: 75 percent / tBuLi; CuBr*Me₂S / tetrahydrofuran / -78 °C

3: 85 percent / MeLi / tetrahydrofuran / -78 °C

4: 84 percent / Zn(Cu) / tetrahydrofuran / -45 °C

5: 87 percent / nBu₃SnH; Et₃B / benzene / Heating

6: 85 percent / p-TsOH / acetone / 20 °C

7: 88 percent / benzene / 20 °C

With n-butyllithium; zinc copper; copper(I) bromide dimethylsulfide complex; triethyl borane; methyllithium; tert.-butyl lithium; tri-n-butyl-tin hydride; toluene-4-sulfonic acid; magnesium bromide; In tetrahydrofuran; acetone; benzene; 4: Marino annulation reaction;
DOI:10.1016/j.tetlet.2006.08.115