(1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

Base Information

Chemical Name:(1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol
CAS No.:161578-83-2
Molecular Formula:C₁₇H₂₄O₇
Molecular Weight:340.373
Hs Code.:

Synonyms:(1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

Chemical Property:

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Technology Process of (1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

There total 3 articles about (1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1-cyclohexene

: 161578-83-2
(1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

Guidance literature:: With potassium osmate(VI); Hydroquinone 1,4-phthalazinediyl diether; methanesulfonamide; water; potassium carbonate; potassium hexacyanoferrate(III); In tert-butyl alcohol; at 0 ℃; for 4h;
DOI:10.1021/ja00105a084

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 161578-83-2
(1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / 23 °C

2: 93 percent / aq. K₂CO₃, K₂OsO₄*2H₂O, K₃Fe(CN)6, (DHQ)2PHAL, CH₃SO₂NH₂ / 2-methyl-propan-2-ol / 4 h / 0 °C

With dmap; potassium osmate(VI); Hydroquinone 1,4-phthalazinediyl diether; methanesulfonamide; potassium carbonate; triethylamine; potassium hexacyanoferrate(III); In dichloromethane; tert-butyl alcohol;
DOI:10.1021/ja00149a003

Reference yield:

: 72445-27-3
(4,4-Dimethoxy-cyclohex-1-enyl)-methanol

: 161578-83-2
(1S,2S)-1-(((4-methoxybenzoyl)oxy)methyl)-4,4-dimethoxy-1,2-cyclohexanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / 23 °C

2: 93 percent / aq. K₂CO₃, K₂OsO₄*2H₂O, K₃Fe(CN)6, (DHQ)2PHAL, CH₃SO₂NH₂ / 2-methyl-propan-2-ol / 4 h / 0 °C

With dmap; potassium osmate(VI); Hydroquinone 1,4-phthalazinediyl diether; methanesulfonamide; potassium carbonate; triethylamine; potassium hexacyanoferrate(III); In dichloromethane; tert-butyl alcohol;
DOI:10.1021/ja00149a003