adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

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Chemical Name:adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester
CAS No.:848771-64-2
Molecular Formula:C₃₆H₄₃NO₅
Molecular Weight:569.741
Hs Code.:

Synonyms:adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

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Chemical Property of adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

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Technology Process of adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

There total 4 articles about adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 62-53-3
aniline

: C₃₀H₃₇O₅⁽¹⁺⁾*ClO₄^(1-)

: 848771-64-2
adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

: adamantane-1-carboxylic acid 2-[2-(2-{4-[3-(4-amino-phenyl)-cyclohepta-1,4,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

Guidance literature:: In dichloromethane; acetonitrile; at 20 ℃; for 5h;
DOI:10.1002/ejoc.200400607

Reference yield:

: 91902-42-0
7-(4-hydroxyphenyl)-1,3,5-cycloheptatriene

: 848771-64-2
adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaOEt / acetonitrile / 0.5 h / 20 °C

1.2: 65 percent / acetonitrile / 4 h / Heating

2.1: 91 percent / pyridine / 4 h / 75 °C

3.1: 67 percent / trityl tetrafluoroborate / CH₂Cl₂

4.1: 20 percent / CH₂Cl₂; acetonitrile / 5 h / 20 °C

With pyridine; sodium ethanolate; trityl tetrafluoroborate; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200400607

Reference yield:

: 848771-62-0
2-{2-[2-(4-cyclohepta-2,4,6-trienyl-phenoxy)-ethoxy]-ethoxy}-ethanol

: 848771-64-2
adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / pyridine / 4 h / 75 °C

2: 67 percent / trityl tetrafluoroborate / CH₂Cl₂

3: 20 percent / CH₂Cl₂; acetonitrile / 5 h / 20 °C

With pyridine; trityl tetrafluoroborate; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200400607