2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

Base Information

Chemical Name:2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate
CAS No.:848771-66-4
Molecular Formula:C₃₆H₄₃NO₅
Molecular Weight:569.741
Hs Code.:

Synonyms:2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

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Chemical Property of 2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

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Technology Process of 2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

There total 6 articles about 2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 848771-64-2
adamantane-1-carboxylic acid 2-[2-(2-{4-[5-(4-amino-phenyl)-cyclohepta-1,3,6-trienyl]-phenoxy}-ethoxy)-ethoxy]-ethyl ester

: 848771-66-4
2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

Guidance literature:: In toluene; for 11h; Heating;
DOI:10.1002/ejoc.200400607

Reference yield:

: 91902-42-0
7-(4-hydroxyphenyl)-1,3,5-cycloheptatriene

: 848771-66-4
2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaOEt / acetonitrile / 0.5 h / 20 °C

1.2: 65 percent / acetonitrile / 4 h / Heating

2.1: 91 percent / pyridine / 4 h / 75 °C

3.1: 67 percent / trityl tetrafluoroborate / CH₂Cl₂

4.1: 20 percent / CH₂Cl₂; acetonitrile / 5 h / 20 °C

5.1: 80 percent / toluene / 11 h / Heating

With pyridine; sodium ethanolate; trityl tetrafluoroborate; In dichloromethane; toluene; acetonitrile;
DOI:10.1002/ejoc.200400607

Reference yield:

: 77544-68-4
8-tosyloxy-3,6-dioxaoctanol

: 848771-66-4
2-[2-(2-{4-[4-(4-aminophenyl)cyclohepta-1,3,5-trienyl]phenoxy}ethoxy)ethoxy]ethyl adamantane-1-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaOEt / acetonitrile / 0.5 h / 20 °C

1.2: 65 percent / acetonitrile / 4 h / Heating

2.1: 91 percent / pyridine / 4 h / 75 °C

3.1: 67 percent / trityl tetrafluoroborate / CH₂Cl₂

4.1: 20 percent / CH₂Cl₂; acetonitrile / 5 h / 20 °C

5.1: 80 percent / toluene / 11 h / Heating

With pyridine; sodium ethanolate; trityl tetrafluoroborate; In dichloromethane; toluene; acetonitrile;
DOI:10.1002/ejoc.200400607