C₆₈H₉₂O₈Si₂

Base Information

Chemical Name:C₆₈H₉₂O₈Si₂
CAS No.:221388-81-4
Molecular Formula:C₆₈H₉₂O₈Si₂
Molecular Weight:1093.64
Hs Code.:

C<sub>68</sub>H<sub>92</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₆₈H₉₂O₈Si₂

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Chemical Property of C₆₈H₉₂O₈Si₂

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Technology Process of C₆₈H₉₂O₈Si₂

There total 11 articles about C₆₈H₉₂O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₈H₉₀O₈Si₂

: 221388-81-4
C₆₈H₉₂O₈Si₂

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.5h; Yield given;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<646::AID-CHEM646>3.0.CO;2-E

Reference yield:

: 221380-85-4
C₄₆H₆₆O₈Si

: 221388-81-4
C₆₈H₉₂O₈Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: 90 percent / KHMDS / tetrahydrofuran; toluene / 2 h / -78 °C

2: 90 percent / LiCl / / tetrahydrofuran / 2 h / 70 °C

3: O₂, tetraphenylporphyrin / CCl₄ / 0.25 h / 25 °C / Irradiation

4: 58 percent / Al(Hg), H₂O, Et₃N / tetrahydrofuran / 2 h / 25 °C

5: 91 percent / imidazole / CH₂Cl₂ / 1 h / 25 °C

6: 82 percent / 4 Angstroem molecular sieves, N-methylmorpholine oxide, TPAP / CH₂Cl₂ / 3 h / 25 °C

7: 70 percent / 3PCuH>6 / benzene / 72 h / 25 °C

8: DIBAL / CH₂Cl₂ / 1 h / -78 °C

9: DMAP / CH₂Cl₂ / 15 h / 40 °C

With 1H-imidazole; dmap; aluminum amalgam; tetrapropylammonium perruthennate; hydrido(triphenylphosphine)copper(I) hexamer; 4 A molecular sieve; water; oxygen; 5,15,10,20-tetraphenylporphyrin; potassium hexamethylsilazane; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; lithium chloride; ; In tetrahydrofuran; tetrachloromethane; dichloromethane; toluene; benzene;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<646::AID-CHEM646>3.0.CO;2-E

Reference yield:

: 221388-51-8
C₅₈H₇₅O₁₁PSi

: 221388-81-4
C₆₈H₉₂O₈Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / LiCl / / tetrahydrofuran / 2 h / 70 °C

2: O₂, tetraphenylporphyrin / CCl₄ / 0.25 h / 25 °C / Irradiation

3: 58 percent / Al(Hg), H₂O, Et₃N / tetrahydrofuran / 2 h / 25 °C

4: 91 percent / imidazole / CH₂Cl₂ / 1 h / 25 °C

5: 82 percent / 4 Angstroem molecular sieves, N-methylmorpholine oxide, TPAP / CH₂Cl₂ / 3 h / 25 °C

6: 70 percent / 3PCuH>6 / benzene / 72 h / 25 °C

7: DIBAL / CH₂Cl₂ / 1 h / -78 °C

8: DMAP / CH₂Cl₂ / 15 h / 40 °C

With 1H-imidazole; dmap; aluminum amalgam; tetrapropylammonium perruthennate; hydrido(triphenylphosphine)copper(I) hexamer; 4 A molecular sieve; water; oxygen; 5,15,10,20-tetraphenylporphyrin; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; lithium chloride; ; In tetrahydrofuran; tetrachloromethane; dichloromethane; benzene;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<646::AID-CHEM646>3.0.CO;2-E