(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

Base Information

Chemical Name:(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate
CAS No.:175849-27-1
Molecular Formula:C₂₇H₃₄O₃S
Molecular Weight:438.631
Hs Code.:

Synonyms:(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

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Chemical Property of (1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

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Technology Process of (1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

There total 5 articles about (1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 79760-22-8
N-<(methylthio)methyl>piperidine hydrochloride

: 115692-74-5
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-oxo-3-phenylpropionate

: 175849-27-1
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

Guidance literature:: In 1,4-dioxane; at 90 ℃; for 17h;
DOI:10.1021/jo9518819

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 175849-27-1
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / Et₃N, DMAP / CH₂Cl₂ / 10 h / Ambient temperature

2: 97 percent / 10percent HCl / methanol / 12 h / Ambient temperature

3: 96 percent / dioxane / 17 h / 90 °C

With hydrogenchloride; dmap; triethylamine; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jo9518819

Reference yield:

: 85892-91-7
2-(2-phenyl-1,3-dioxolan-2-yl)acetic acid

: 175849-27-1
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylthio)methyl>-3-oxo-3-phenylpropionate

Guidance literature:: Multi-step reaction with 4 steps

1: (COCl)2 / benzene / 3 h / Ambient temperature

2: 83 percent / Et₃N, DMAP / CH₂Cl₂ / 10 h / Ambient temperature

3: 97 percent / 10percent HCl / methanol / 12 h / Ambient temperature

4: 96 percent / dioxane / 17 h / 90 °C

With hydrogenchloride; dmap; oxalyl dichloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane; benzene;
DOI:10.1021/jo9518819