C₂₆H₃₀INO₃

Base Information

Chemical Name:C₂₆H₃₀INO₃
CAS No.:1253215-90-5
Molecular Formula:C₂₆H₃₀INO₃
Molecular Weight:531.434
Hs Code.:

C<sub>26</sub>H<sub>30</sub>INO<sub>3</sub>

Synonyms:C₂₆H₃₀INO₃

Suppliers and Price of C₂₆H₃₀INO₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₆H₃₀INO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₆H₃₀INO₃

There total 9 articles about C₂₆H₃₀INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1253215-89-2
C₂₆H₃₁NO₃

: 1253215-90-5
C₂₆H₃₀INO₃

Guidance literature:: With iodine; silver(I) acetate; In dichloromethane; at 20 ℃; for 5h; Darkness;

Reference yield:

: 939430-71-4
6-chloro-5-methoxymethoxy-pyridine-2-carbaldehyde

: 1253215-90-5
C₂₆H₃₀INO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 11 h / 90 °C / Inert atmosphere

3.1: pyridine / 6.5 h

4.1: palladium 10% on activated carbon; hydrogen / acetic acid; ethyl acetate / 14 h

5.1: acetic acid / ethanol / 15 h / 20 - 50 °C

6.1: caesium carbonate / acetonitrile / 2 h

7.1: iodine; silver(I) acetate / dichloromethane / 5 h / 20 °C / Darkness

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; hydrogen; iodine; silver(I) acetate; caesium carbonate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; acetonitrile;

Reference yield:

: 848442-41-1
C₁₂H₁₇BrO₂

: 1253215-90-5
C₂₆H₃₀INO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 11 h / 90 °C / Inert atmosphere

3.1: pyridine / 6.5 h

4.1: palladium 10% on activated carbon; hydrogen / acetic acid; ethyl acetate / 14 h

5.1: acetic acid / ethanol / 15 h / 20 - 50 °C

6.1: caesium carbonate / acetonitrile / 2 h

7.1: iodine; silver(I) acetate / dichloromethane / 5 h / 20 °C / Darkness

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; hydrogen; iodine; silver(I) acetate; caesium carbonate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; acetonitrile;