benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

Base Information

Chemical Name:benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt
CAS No.:131150-08-8
Molecular Formula:C₁₉H₂₉O₁₄P*H₃N
Molecular Weight:529.435
Hs Code.:

Synonyms:benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

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Chemical Property of benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

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Technology Process of benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

There total 9 articles about benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 131166-78-4
benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

: 131150-08-8
benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

Guidance literature:: With sodium methylate; In 1,4-dioxane; methanol; at 1 ℃; for 4h;
DOI:10.1016/0008-6215(90)84021-L

Reference yield:

: 26531-92-0
3-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 131150-08-8
benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / pyridine

2: 92 percent / aq. 70percent acetic acid / 70 °C

3: 97 percent / pyridine

4: 85 percent / acetyl chloride / methanol / 20 °C

6: 88 percent / 0.1M MeONa / methanol; dioxane / 4 h / 1 °C

With pyridine; sodium methylate; acetic acid; acetyl chloride; In 1,4-dioxane; methanol;
DOI:10.1016/0008-6215(90)84021-L

Reference yield:

: 131150-16-8
benzyl 2-O-acetyl-3-O-benzoyl-β-D-galactopyranoside

: 131150-08-8
benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / pyridine

2: 85 percent / acetyl chloride / methanol / 20 °C

4: 88 percent / 0.1M MeONa / methanol; dioxane / 4 h / 1 °C

With pyridine; sodium methylate; acetyl chloride; In 1,4-dioxane; methanol;
DOI:10.1016/0008-6215(90)84021-L