benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

Base Information

Chemical Name:benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt
CAS No.:131166-78-4
Molecular Formula:C₆H₁₅N*C₆₈H₅₇O₂₁P
Molecular Weight:1342.35
Hs Code.:

Synonyms:benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

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Chemical Property of benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

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Technology Process of benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

There total 7 articles about benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26531-92-0
3-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 131166-78-4
benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / pyridine

2: 92 percent / aq. 70percent acetic acid / 70 °C

3: 97 percent / pyridine

4: 85 percent / acetyl chloride / methanol / 20 °C

With pyridine; acetic acid; acetyl chloride; In methanol;
DOI:10.1016/0008-6215(90)84021-L

Reference yield:

: 131150-16-8
benzyl 2-O-acetyl-3-O-benzoyl-β-D-galactopyranoside

: 131166-78-4
benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / pyridine

2: 85 percent / acetyl chloride / methanol / 20 °C

With pyridine; acetyl chloride; In methanol;
DOI:10.1016/0008-6215(90)84021-L

Reference yield:

: 131150-15-7
benzyl 2-O-acetyl-3-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 131166-78-4
benzyl 3,4,6-tri-O-benzoyl-β-D-galactopyranoside 2-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl phosphate), triethylammonium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / aq. 70percent acetic acid / 70 °C

2: 97 percent / pyridine

3: 85 percent / acetyl chloride / methanol / 20 °C

With pyridine; acetic acid; acetyl chloride; In methanol;
DOI:10.1016/0008-6215(90)84021-L