[2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Base Information

• Chemical Name: [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl
• CAS No.: 955094-78-7
• Molecular Formula: C₃₁H₁₂Cl₁₀N
• Molecular Weight: 752.973
• Mol file: 955094-78-7.mol

Synonyms:[2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Chemical Property of [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

There total 3 articles about [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

[2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-72-1) → [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl (955094-78-7)

Guidance literature:

[2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane; With sodium hydroxide; In diethyl ether; dimethyl sulfoxide; at 20 ℃; for 48h;

With iodine; In diethyl ether; dimethyl sulfoxide; for 2h; Further stages.;

DOI:10.1021/jo0708846

Reference yield: 43.0%

(4-(N-carbazolyl)-2,6-dichlorophenyl)bis(2,4,6-trichlorophenyl)methyl radical (881917-48-2) → [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl (955094-78-7)

Guidance literature:

With sulfuryl dichloride; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo0708846

Reference yield:

[4-(N-carbazolyl)-2,6-dichlorophenyl]bis(2,4,6-trichlorophenyl)methane (881917-50-6) → [2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl (955094-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 81 percent / sulfuryl chloride / CH₂Cl₂ / 0 - 20 °C

2.1: sodium hydroxide / diethyl ether; dimethylsulfoxide / 48 h / 20 °C

2.2: 72 percent / iodine / diethyl ether; dimethylsulfoxide / 2 h

With sodium hydroxide; sulfuryl dichloride; In diethyl ether; dichloromethane; dimethyl sulfoxide;

DOI:10.1021/jo0708846

upstream raw materials:

(4-(N-carbazolyl)-2,6-dichlorophenyl)bis(2,4,6-trichlorophenyl)methyl radical

[2,6-dichloro-4-(3,6-dichloro-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

[4-(N-carbazolyl)-2,6-dichlorophenyl]bis(2,4,6-trichlorophenyl)methane