(2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

Base Information

Chemical Name:(2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol
CAS No.:1009605-87-1
Molecular Formula:C₁₆H₁₈F₃NO₂
Molecular Weight:313.32
Hs Code.:

Synonyms:(2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

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Chemical Property of (2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

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Technology Process of (2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

There total 1 articles about (2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1009605-77-9
(R)-3-(pent-4-enyl)-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 1009605-87-1
(2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1021/ol702947n

Reference yield: 83.0%

: 1009605-87-1
(2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

: 1009606-68-1
(1R,4R,6S)-6-(iodomethyl)-4-phenyl-1-(trifluoromethyl)-1,3,4,6,7,8-hexahydropyrido[2,1-c][1,4]oxazin-1-ol

Guidance literature:: With iodine; In chloroform; at 20 ℃; for 3h;
DOI:10.1021/ol702947n

Reference yield: 80.0%

: 1009605-87-1
(2R,5R)-3-(pent-4-enyl)-5-phenyl-2-(trifluoromethyl)-5,6-dihydro-2H-1,4-oxazin-2-ol

: 1009606-69-2
C₁₆H₁₆F₃I₂NO₂

Guidance literature:: With iodine; sodium hydride; In tetrahydrofuran; at 60 ℃; for 0.5h; stereoselective reaction; Inert atmosphere; Microwave irradiation;
DOI:10.1002/chem.201102351