N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide)

Base Information

• Chemical Name: N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide)
• CAS No.: 1415392-93-6
• Molecular Formula: C₁₂H₁₈F₆N₂O₄
• Molecular Weight: 368.276

Synonyms:N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide)

Chemical Property of N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide)

Chemical Property:

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Technology Process of N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide)

There total 3 articles about N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

-butyl vinyl ether (111-34-2,92680-80-3) + N-(3-hydroxypropyl)trifluoroacetamide (78008-15-8) → dibutyl acetal (871-22-7) + N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide) (1415392-93-6) + N-[3-(1-butoxyethoxy)propyl]-2,2,2-trifluoroacetamide (1415392-89-0)

Guidance literature:

With hydrogenchloride; In diethyl ether; for 3 - 11h; Reflux;

DOI:10.1134/S1070428012100053

Reference yield: 74.0%

2,2,2-trifluoro-N-[3-(vinyloxy)propyl]acetamide (1339837-81-8) → N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide) (1415392-93-6) + N-(3-hydroxypropyl)trifluoroacetamide (78008-15-8)

Guidance literature:

With phosphoric acid; In toluene; for 11h; Reflux;

DOI:10.1134/S107042801507026X

Reference yield: 56.0%

N-(3-hydroxypropyl)trifluoroacetamide (78008-15-8) + ethyl vinyl ether (109-92-2,25104-37-4) → diethyl acetal (105-57-7,30846-29-8) + N,N′-[ethane-1,1-diylbis(oxypropane-3,1-diyl)]bis(2,2,2-trifluoroacetamide) (1415392-93-6) + N-[3-(1-ethoxyethoxy)propyl]-2,2,2-trifluoroacetamide (1415392-88-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; for 3 - 11h; Reflux;

DOI:10.1134/S1070428012100053

upstream raw materials:

N-(3-hydroxypropyl)trifluoroacetamide

ethyl vinyl ether

-butyl vinyl ether

2,2,2-trifluoro-N-[3-(vinyloxy)propyl]acetamide

Downstream raw materials:

2,2,2-trifluoro-N-[3-(vinyloxy)propyl]acetamide

N-(3-hydroxypropyl)trifluoroacetamide

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