N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

Base Information

Chemical Name:N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane
CAS No.:479251-85-9
Molecular Formula:C₂₁H₂₉N₅O
Molecular Weight:367.494
Hs Code.:

Synonyms:N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

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Chemical Property of N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

Chemical Property:

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Technology Process of N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

There total 6 articles about N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-((1R,3S,5R)-3,5-Bis-{[1-pyridin-2-yl-meth-(E)-ylidene]-amino}-cyclohexyl)-propionamide

: 479251-85-9
N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 24h;
DOI:10.1021/jo0204911

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 479251-85-9
N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 4 h / Heating

2: 415 mg / NaBH₄ / ethanol / 24 h / 20 °C

With sodium tetrahydroborate; In ethanol;
DOI:10.1021/jo0204911

Reference yield:

: 26150-46-9
cis,cis-1,3,5-triaminocyclohexane

: 479251-85-9
N,N'-bis(2-pyridylmethyl)-N''-propionyl-cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / CHCl₃ / 2 h / Heating

2: 51 percent / Et₃N / CH₂Cl₂ / 0.17 h / -20 °C

3: 80 percent / CF₃CO₂H / CHCl₃; methanol / 48 h / -5 - 20 °C

4: ethanol / 4 h / Heating

5: 415 mg / NaBH₄ / ethanol / 24 h / 20 °C

With sodium tetrahydroborate; triethylamine; trifluoroacetic acid; In methanol; ethanol; dichloromethane; chloroform;
DOI:10.1021/jo0204911