C₁₄H₁₅N₃O

Base Information

• Chemical Name: C₁₄H₁₅N₃O
• CAS No.: 52416-30-5
• Molecular Formula: C₁₄H₁₅N₃O
• Molecular Weight: 241.293
• Mol file: 52416-30-5.mol

Synonyms:C₁₄H₁₅N₃O

Chemical Property of C₁₄H₁₅N₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₅N₃O

There total 3 articles about C₁₄H₁₅N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4-phenoxybenzene-1-diazonium tetrafluoroborate + N,N-dimethyl-formamide (68-12-2,33513-42-7) → C14H15N3O (52416-30-5)

Guidance literature:

With caesium carbonate; phenylpropyolic acid; In methanol; at 60 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.tet.2021.132185

Reference yield:

4-phenoxyanilin (139-59-3) → C14H15N3O (52416-30-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tert.-butylnitrite / methanol / -20 - 20 °C / Schlenk technique; Inert atmosphere

2: phenylpropyolic acid; caesium carbonate / methanol / 60 °C / Inert atmosphere; Schlenk technique

With tert.-butylnitrite; caesium carbonate; phenylpropyolic acid; In methanol;

DOI:10.1016/j.tet.2021.132185

Reference yield:

→ C14H15N3O (52416-30-5)

Guidance literature:

aus Diazoniumsalz, sec. Amin;

upstream raw materials:

N,N-dimethyl-formamide

4-phenoxyanilin