2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

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Chemical Name:2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane
CAS No.:201424-73-9
Molecular Formula:C₃₇H₃₄N₂O₆
Molecular Weight:602.687
Hs Code.:

Synonyms:2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

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Chemical Property of 2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

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Technology Process of 2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

There total 6 articles about 2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 201424-72-8
(-)-N,N'-bis[(2S,3S)-(3-phenylcarboxy-3-phenyl-1-chloropropyl)]-2,2-dimethyl-1,3-propanediamine

: 201424-73-9
2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

Guidance literature:: With triethylamine; In toluene; Heating;
DOI:10.1016/S0957-4166(97)00499-0

Reference yield:

: 28143-91-1
(1S,2S)-2-amino-1-phenyl-1,3-diol

: 201424-73-9
2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / Et₃N / CH₂Cl₂ / 15 h / Ambient temperature

2: 2 M aq. HCl / tetrahydrofuran / 24 h / Ambient temperature

3: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

4: SOCl₂ / CH₂Cl₂ / 3 h / Heating

5: 83 percent / Et₃N / toluene / Heating

With hydrogenchloride; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0957-4166(97)00499-0

Reference yield:

: 5333-86-8
ethyl benzimidate hydrochloride

: 201424-73-9
2,2-bis-{2-[(4S)-((1S)-1-phenylcarboxy-1-phenylmethyl)-1,3-oxazolinyl]}propane

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / Et₃N / CH₂Cl₂ / 15 h / Ambient temperature

2: 2 M aq. HCl / tetrahydrofuran / 24 h / Ambient temperature

3: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

4: SOCl₂ / CH₂Cl₂ / 3 h / Heating

5: 83 percent / Et₃N / toluene / Heating

With hydrogenchloride; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0957-4166(97)00499-0