(S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

Base Information

Chemical Name:(S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol
CAS No.:201424-74-0
Molecular Formula:C₂₃H₂₆N₂O₄
Molecular Weight:394.47
Hs Code.:

Synonyms:(S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

There total 6 articles about (S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28143-91-1
(1S,2S)-2-amino-1-phenyl-1,3-diol

: 201424-74-0
(S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / Et₃N / CH₂Cl₂ / 15 h / Ambient temperature

2: 2 M aq. HCl / tetrahydrofuran / 24 h / Ambient temperature

3: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

4: SOCl₂ / CH₂Cl₂ / 3 h / Heating

5: 83 percent / Et₃N / toluene / Heating

6: 190 mg / 1percent methanol. NaOH / 0.5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0957-4166(97)00499-0

Reference yield:

: 95341-86-9
(+)-(4,5-dihydro-2,5-diphenyloxazol-4-yl)methanol

: 201424-74-0
(S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: 2 M aq. HCl / tetrahydrofuran / 24 h / Ambient temperature

2: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

3: SOCl₂ / CH₂Cl₂ / 3 h / Heating

4: 83 percent / Et₃N / toluene / Heating

5: 190 mg / 1percent methanol. NaOH / 0.5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0957-4166(97)00499-0

Reference yield:

: Benzoic acid (1S,2S)-2-amino-3-hydroxy-1-phenyl-propyl ester; hydrochloride

: 201424-74-0
(S)-((S)-2-{1-[(S)-4-((S)-Hydroxy-phenyl-methyl)-4,5-dihydro-oxazol-2-yl]-1-methyl-ethyl}-4,5-dihydro-oxazol-4-yl)-phenyl-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

2: SOCl₂ / CH₂Cl₂ / 3 h / Heating

3: 83 percent / Et₃N / toluene / Heating

4: 190 mg / 1percent methanol. NaOH / 0.5 h / Ambient temperature

With sodium hydroxide; thionyl chloride; triethylamine; In dichloromethane; toluene;
DOI:10.1016/S0957-4166(97)00499-0