Technology Process of C22H28N6O5
There total 8 articles about C22H28N6O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 25 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 16 h / 100 °C
2: 4 h
3: tert-butyl alcohol / 16 h / 80 °C
4: trifluoroacetic acid / dichloromethane / 16 h / 25 °C
With
N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl acetamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thiophene; hydrogen / palladium 10% on activated carbon / ethanol; di-isopropyl ether / 20 °C
2: hydrogenchloride; water / 1,4-dioxane / 20 - 50 °C
3: tert-butyl alcohol / 16 h / 80 °C
4: trifluoroacetic acid / dichloromethane / 16 h / 25 °C
With
thiophene; hydrogenchloride; water; hydrogen; trifluoroacetic acid;
palladium 10% on activated carbon;
In
1,4-dioxane; ethanol; dichloromethane; di-isopropyl ether; tert-butyl alcohol;