4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

Base Information

Chemical Name:4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene
CAS No.:1207993-63-2
Molecular Formula:C₁₇H₂₄O₂S
Molecular Weight:292.442
Hs Code.:

Synonyms:4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

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Technology Process of 4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

There total 1 articles about 4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1207993-60-9
2-acetoxy-4-tert-butyl-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

: 1207993-63-2
4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo902477n

Reference yield: 83.0%

: 1207993-63-2
4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

: 74-88-4
methyl iodide

: 1207993-61-0
4-tert-butyl-2-methoxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene

Guidance literature:: 4-tert-butyl-2-hydroxy-5-(3-methoxyphenyl)-3,3-dimethyl-2,3-dihydrothiophene; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; for 1h;
DOI:10.1021/jo902477n