chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide

Base Information

Chemical Name:chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide
CAS No.:94780-58-2
Molecular Formula:C₄₄H₃₆ClIO₂OsP₃*I
Molecular Weight:1169.15
Hs Code.:

Synonyms:chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide

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Chemical Property of chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide

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Technology Process of chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide

There total 2 articles about chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 93366-11-1
C₄₄H₃₆ClO₂OsP₃

: 94780-58-2
chloro(phenyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) iodide

Guidance literature:: With I₂; In benzene; N2-atmosphere; dropwise addn. of benzene soln. of I2 to suspn. of Os-complex in benzene; stirring for 10 min;; filtration; washing with hexane; recrystn. from CH2Cl2/hexane; elem. anal.;

Reference yield:

: 93366-11-1
osmium(Cl)(PHPh)(CO)2(PPh₃)2

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 94780-58-2
{Os(PHIC₆H₅)Cl(CO)2(P(C₆H₅)3)2}⁽¹⁺⁾*I^(1-)={Os(PHIC₆H₅)Cl(CO)2(P(C₆H₅)3)2}I

Guidance literature:: In not given; detn. by IR and (1)H-NMR;;
DOI:10.1016/0022-328X(84)80514-8

Reference yield:

: 94780-58-2
{Os(PHIC₆H₅)Cl(CO)2(P(C₆H₅)3)2}⁽¹⁺⁾*I^(1-)={Os(PHIC₆H₅)Cl(CO)2(P(C₆H₅)3)2}I

: 94780-59-3
{Os(PIC₆H₅)Cl(CO)2(P(C₆H₅)3)2}

Guidance literature:: With 1,8-diazabicyclo{5.4.0}undec-7-ene; In neat (no solvent); recrystn. form benzene/methanol; elem. anal.; detn. by IR;;
DOI:10.1016/0022-328X(84)80514-8