methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

Base Information

Chemical Name:methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate
CAS No.:1200833-53-9
Molecular Formula:C₂₈H₂₈Cl₃NO₁₀
Molecular Weight:644.89
Hs Code.:

Synonyms:methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

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Chemical Property of methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

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Technology Process of methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

There total 15 articles about methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₂₈O₁₀

: 545-06-2
trichloroacetonitrile

: 1200833-53-9
methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃;

Reference yield:

: C₂₆H₂₇IO₉

: 545-06-2
trichloroacetonitrile

: 1200833-53-9
methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/jo400467g

Reference yield:

: 100-39-0
benzyl bromide

: 1200833-53-9
methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α/β-L-idopyranosyluronate trichloroacetimidate

Guidance literature:: Multi-step reaction with 12 steps

1: sodium hydride / tetrahydrofuran

2: acetic acid / tetrahydrofuran

3: sodium periodate

4: tetrahydrofuran / -78 °C

5: trifluoroacetic acid; water

6: camphor-10-sulfonic acid

7: dmap; diisopropyl-carbodiimide / dichloromethane / 0 - 20 °C / Darkness

8: trifluoroacetic acid; water / 1 h

9: 1H-imidazole / dichloromethane / 20 °C

10: pyridine / dichloromethane / 0 - 8 °C / Inert atmosphere

11: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 °C

12: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C

With pyridine; 1H-imidazole; dmap; sodium periodate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; water; sodium hydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;