(R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

Base Information

Chemical Name:(R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide
CAS No.:441788-44-9
Molecular Formula:C₁₇H₂₇NO₂S
Molecular Weight:309.473
Hs Code.:

(R<sub>S</sub>,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

Synonyms:(R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

Suppliers and Price of (R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

Chemical Property:

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Technology Process of (R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

There total 2 articles about (R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 630-19-3
pivalaldehyde

: 220263-59-2
(R_S)-2-methyl-N-(1-phenylethylidene)propane-2-sulfinamide

: 441788-44-9
(R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

Guidance literature:: (R_S)-2-methyl-N-(1-phenylethylidene)propane-2-sulfinamide; With lithium diisopropyl amide; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

With magnesium bromide; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

pivalaldehyde; In tetrahydrofuran; pentane; at -78 ℃; for 3h; Further stages.;
DOI:10.1021/ja026292g

Reference yield:

: 630-19-3
pivalaldehyde

: 220263-59-2
(R_S)-2-methyl-N-(1-phenylethylidene)propane-2-sulfinamide

: 441788-44-9
(R_S,S)-N-(3-hydroxy-4,4-dimethyl-1-phenylpentylidene)-tert-butanesulfinamide

: 2-Methyl-propane-2-sulfinic acid [(R)-3-hydroxy-4,4-dimethyl-1-phenyl-pent-(E)-ylidene]-amide

Guidance literature:: (R_S)-2-methyl-N-(1-phenylethylidene)propane-2-sulfinamide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

With magnesium bromide; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

pivalaldehyde; In tetrahydrofuran; pentane; at -78 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1021/ja0363462