C₁₇H₁₆F₃NO₇S

Base Information

Chemical Name:C₁₇H₁₆F₃NO₇S
CAS No.:1268261-69-3
Molecular Formula:C₁₇H₁₆F₃NO₇S
Molecular Weight:435.378
Hs Code.:

C<sub>17</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>7</sub>S

Synonyms:C₁₇H₁₆F₃NO₇S

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Chemical Property of C₁₇H₁₆F₃NO₇S

Chemical Property:

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Technology Process of C₁₇H₁₆F₃NO₇S

There total 1 articles about C₁₇H₁₆F₃NO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1268261-68-2
C₁₆H₁₇NO₅

: 1268261-69-3
C₁₇H₁₆F₃NO₇S

Guidance literature:: C₁₆H₁₇NO₅; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 3h; Inert atmosphere;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1002/anie.201006367

Reference yield: 83.0%

: 1268261-70-6
C₁₅H₁₇BO₅

: 1268261-69-3
C₁₇H₁₆F₃NO₇S

: 1268261-71-7
C₃₁H₃₁NO₇

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 70 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/anie.201006367

Reference yield:

: 1268261-69-3
C₁₇H₁₆F₃NO₇S

: 1268261-64-8
C₂₅H₂₅NO₆S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 2.5 h / 70 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 1.5 h / 25 °C

3: pyridine / dichloromethane / 12 h / 25 °C / Inert atmosphere

4: 20% palladium(II) hydroxide on carbon; hydrogen / ethyl acetate / 1.5 h / 25 °C

5: water; acetic acid / 20 h / 25 °C / Inert atmosphere

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20% palladium(II) hydroxide on carbon; palladium 10% on activated carbon; water; hydrogen; sodium carbonate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; 1: Suzuki-Miyaura reaction;
DOI:10.1002/anie.201006367