Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

Base Information

Chemical Name:Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate
CAS No.:73838-90-1
Molecular Formula:C₁₅H₁₇NO₄
Molecular Weight:275.304
Hs Code.:

Synonyms:Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

There total 1 articles about Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6213-87-2
methyl (2E)-3-bromoacrylate

: 40216-71-5
methyl 2-(benzylideneamino)propanoate

: 73838-90-1
Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1) THF, 30 min -70 deg C 2) 2h 20 deg C;
DOI:10.1021/jo01304a021

Reference yield:

: 73838-90-1
Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

: 71-90-9,470-51-9
2-methylglutamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 3M aqueous HCl 2) propylene oxide / 1) ether, 24h 60 deg C 2) methanol

2: catalytic hydrogenation

With hydrogenchloride; methyloxirane;
DOI:10.1021/jo01304a021

Reference yield:

: 73838-90-1
Dimethyl (E)-2-(benzylideneamino)-2-methylpent-3-ene-2,5-dioate

: 73838-85-4,71897-84-2
α-methyl-(E)-3,4-dehydroglutamic acid

Guidance literature:: With hydrogenchloride; methyloxirane; Yield given. Multistep reaction; 1) ether, 24h 60 deg C 2) methanol;
DOI:10.1021/jo01304a021